A practical guide to structural analysis of carbohydrates
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A practical guide to structural analysis of carbohydrates
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Structural analysis
Introduction
Component analysis
Sugar analysis
Using morpholinoborane
Using trifluoroacetates
Solvolysis with HF
Solvolysis with Methanol
Linkage analysis
Methylation - DMSO
Methylation of LOS
Methyl iodide/NaOH
Carboxyl reduction 1
Carboxyl reduction 2
Dimsyl sodium
Specific degradations
Smith degradation
Uronic acid degradation
Absolute configuration
Silylated butyl glycosides
Acetylated butyl glycosides
Purification
Delipidation of LPS
Phenol-water extraction
RNAse treatment
Protease treatment
Removal of phospholipids
Various procedures
Fatty acid analysis
Protein content
Phosphorous content
Appendix
Aldoses
Pentoses
Hexoses
Ketoses
Alditols
Chemical shifts
Coupling constants
Occurence
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